High Temperature Drift Spectra Measurements

Mirostaw Handke; Kazimierz Czarnecki

doi:10.1117/12.969579

1 December 1989 High Temperature Drift Spectra Measurements

Mirostaw Handke, Kazimierz Czarnecki

Proceedings Volume 1145, 7th Intl Conf on Fourier Transform Spectroscopy; (1989) https://doi.org/10.1117/12.969579
Event: Seventh International Conference on Fourier and Computerized Infrared Spectroscopy, 1989, Fairfax, VA, United States

Abstract

There are many problems in the chemistry of solids which can be solved by "in situ" high temperature IR spectra measurement. Such a measurements should be very helpful in the studies of: phase transition, formation and decomposition of solids, adsorption on solid surfaces, oxidation or reduction reaction, to name a few. Among sampling techniques used in IR spectroscopy the transmission, diffuse reflection and emission seems be useful for high temperature IR spectra measurement. The main aim of the presented paper is to show the great potential of DRIFT technique in high temperature spectra measurements under controled atmosphere. The paper also show how DRIFT accessory can be used for IR emission spectra measurements as well. The following problems solved with high temperature DRIFT technique will be discussed in the paper: - Si02 polymorphic transition - desorption of the water molecules from quartz surface, - molybdenium and vanadium oxides reduction, - phosphor - molybdenium heteropolyacid catalyst reactions. Some experimental problems concerning the high temperature DRIFT measurements will be discussed also.

Citation Download Citation

Mirostaw Handke and Kazimierz Czarnecki "High Temperature Drift Spectra Measurements", Proc. SPIE 1145, 7th Intl Conf on Fourier Transform Spectroscopy, (1 December 1989); https://doi.org/10.1117/12.969579

ACCESS THE FULL ARTICLE

INSTITUTIONAL
Select your institution to access the SPIE Digital Library.

SELECT YOUR INSTITUTION

PERSONAL
Sign in with your SPIE account to access your personal subscriptions or to use specific features such as save to my library, sign up for alerts, save searches, etc.

PERSONAL SIGN IN

No SPIE Account? Create one

PURCHASE THIS CONTENT

SUBSCRIBE TO DIGITAL LIBRARY

50 downloads per 1-year subscription

Members: $195

Non-members: $335 ADD TO CART

25 downloads per 1 - year subscription

Members: $145

Non-members: $250 ADD TO CART

PURCHASE SINGLE ARTICLE

Includes PDF, HTML & Video, when available