Tracking of the organic species during the synthesis of cobalt-based nanoparticles in non-aqueous solution

M. Staniuk; M. Niederberger; D. Koziej

doi:10.1117/12.2060064

28 August 2014 Tracking of the organic species during the synthesis of cobalt-based nanoparticles in non-aqueous solution

M. Staniuk, M. Niederberger, D. Koziej

Author Affiliations +

Proceedings Volume 9170, Nanoengineering: Fabrication, Properties, Optics, and Devices XI; 91700E (2014) https://doi.org/10.1117/12.2060064
Event: SPIE NanoScience + Engineering, 2014, San Diego, California, United States

Abstract

In this work we investigate the organic products of the synthesis of Co-based nanoparticles in benzyl alcohol. Our GC and in situ IR studies provide the experimental proofs for the formation of benzaldehyde, toluene and isopropanol in the reaction solution. These organic products can be correlated with formation of cobalt-based nanoparticles with oxidation state from 0 to 3+. These results shine the light on the complexity of organic and inorganic reactions in solution during crystallization of nanoparticles.

Citation Download Citation

M. Staniuk, M. Niederberger, and D. Koziej "Tracking of the organic species during the synthesis of cobalt-based nanoparticles in non-aqueous solution", Proc. SPIE 9170, Nanoengineering: Fabrication, Properties, Optics, and Devices XI, 91700E (28 August 2014); https://doi.org/10.1117/12.2060064

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