Paper
10 December 2001 Efficiency calibration of the four multilayer-coated holographic ion-etched flight gratings for a sounding rocket high-resolution spectrometer
Michael P. Kowalski, Herbert Gursky, Jack C. Rife, Daryl J. Yentis, Raymond G. Cruddace, Troy W. Barbee Jr., William H. Goldstein, Joseph F. Kordas, Klaus F. Heidemann, Gilbert G. Fritz, William R. Hunter, Martin Adrian Barstow, George W. Fraser, Nigel P. Bannister, Jonathan S. Lapington, J. A. Tandy, B. S. Sanderson
Author Affiliations +
Abstract
We have fabricated the four flight gratings for a sounding rocket high-resolution spectrometer using a holographic ion-etching technique. The gratings are spherical (4000-mm radius of curvature), large (160 mm x 90 mm), and have a laminar groove profile of high density (3600 grooves/mm). They have been coated with a high-reflectance multilayer of Mo5C/Si/Mo2Si. Using an atomic force microscope, we examined the surface characteristics before and after multilayer coating. The average roughness is approximately 2-3A rms after coating, somewhat smoothened by the multilayer. Using synchrotron radiation, we completed an efficiency calibration map of each grating over the wavelength range 225-245A. At an angle of incidence of 5 degree(s) and a wavelength of 234A, the average efficiency peaks in the first inside order at 10.3+/- 0.6% for Grating 1, 7.3+/- 0.9% for Grating 6, 7.2+/- 1.2% for Grating 3, and 9.0+/- 1.5% for Grating 4. These values exceed all previously published results for a high density grating. The first order groove efficiency for Grating 1 is 34.4+/- 1.9%, in good agreement with the best value obtained from similar test gratings and close to the theoretical limit of 40.5%.
© (2001) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.
Michael P. Kowalski, Herbert Gursky, Jack C. Rife, Daryl J. Yentis, Raymond G. Cruddace, Troy W. Barbee Jr., William H. Goldstein, Joseph F. Kordas, Klaus F. Heidemann, Gilbert G. Fritz, William R. Hunter, Martin Adrian Barstow, George W. Fraser, Nigel P. Bannister, Jonathan S. Lapington, J. A. Tandy, and B. S. Sanderson "Efficiency calibration of the four multilayer-coated holographic ion-etched flight gratings for a sounding rocket high-resolution spectrometer", Proc. SPIE 4498, UV/EUV and Visible Space Instrumentation for Astronomy and Solar Physics, (10 December 2001); https://doi.org/10.1117/12.450065
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Cited by 3 scholarly publications.
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KEYWORDS
Multilayers

Coating

Atomic force microscopy

Calibration

Spectroscopy

Holography

Reflectivity

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