Process development utilizing advanced technologies: the RC1 reaction calorimeter, the multifunctional SimuSolv software, and the ReactIR reaction analysis system

Ralph N. Landau; Susan M. Penix; Steven M. Donahue; Alan J. Rein

doi:10.1117/12.137756

14 August 1992 Process development utilizing advanced technologies: the RC1 reaction calorimeter, the multifunctional SimuSolv software, and the ReactIR reaction analysis system

Ralph N. Landau, Susan M. Penix, Steven M. Donahue, Alan J. Rein

Author Affiliations +

Proceedings Volume 1681, Optically Based Methods for Process Analysis; (1992) https://doi.org/10.1117/12.137756
Event: SPIE's 1992 Symposium on Process Control and Monitoring, 1992, Somerset, NJ, United States

Abstract

In-situ FTIR has been used to monitor reactions occurring in an automated laboratory calorimeter. The study successfully acquired both Arrhenius parameters and heats of reaction from a single experiment. The combination of enhanced control and measurement sensitivity affords an efficient method of reaction monitoring and process development. In addition to providing composition monitoring, the FTIR-based analysis system revealed reaction pathway information. The highly controllable automated laboratory calorimeter accurately and precisely regulated and recorded reaction conditions leading to the estimation of model parameters with high confidence.

Citation Download Citation

Ralph N. Landau, Susan M. Penix, Steven M. Donahue, and Alan J. Rein "Process development utilizing advanced technologies: the RC1 reaction calorimeter, the multifunctional SimuSolv software, and the ReactIR reaction analysis system", Proc. SPIE 1681, Optically Based Methods for Process Analysis, (14 August 1992); https://doi.org/10.1117/12.137756

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