This study focus on the analysis of various plastic samples using the portable MEMS-FTIR spectrometer in both transmission and diffuse reflection modes operating at two resolutions of 10 nm and 16 nm. The analysis focuses on the mid-infrared region spanning from 2000 nm to 4600 nm. Many plastic samples have been differentiated such as Nylon, Polypropylene, Polystyrene, Acrylonitrile butadiene styrene, and colored High-Density Polyethylene. The results shows that transmission module is efficient for clear plastic samples sorting and diffused reflection module is efficient for opaque plastic samples sorting. The findings position the MEMS-FTIR spectrometer as a portable, cost-effective, and accurate solution for plastic analysis tasks, demonstrating versatility and potential advantages over traditional methods in the specified MIR range.
Air pollution is used to refer to the release of pollutants into the air, where these pollutants are harmful to the human health and our planet. The main source of these pollutants comes from energy production and consumption that release Volatile Organic Compounds (VOCs) such as BTEX and Aldehydes group. Real time monitoring of these VOCs in factories, stations, homes and in the street is important for analysis of the pollution sources fingerprint and for alerting, when exceeding the harmful limits. In this work we report the use of a MEMS FTIR spectrometer in the mid-infrared for this purpose. The spectrometer works in the wavelength range of 1.6 μm - 4.9 μm with a resolution down to 33 cm-1. This covers the absorption spectrum of water vapour, BTEX, Aldehydes and CO2 around 2.65 μm, 3.27 μm, 3.6 μm and 4.3 μm, respectively. The spectra of Toluene with different concentrations are measured, using a multipass gas cell with a physical length of 50 cm and an optical path length of 20 m, showing excellent sensor linearity. The minimum concentration measured is 350 ppb limited by the interference of the side lobes of the strong absorption of water vapour, which can be overcome in the future by humidity compensation. The SNR is measured and found to be 5000:1, corresponding to a detection limit of about 90 ppb. The achieved results open the door for a compact and low-cost solution targeting air pollution monitoring.
Portable and handheld spectrometers are being developed and commercialized in the late few years leveraging the rapidly-progressing technology and triggering new markets in the field of on-site spectroscopic analysis. Although handheld devices were commercialized for the near-infrared spectroscopy (NIRS), their size and cost stand as an obstacle against the deployment of the spectrometer as spectral sensing components needed for the smart phone industry and the IoT applications. In this work we report a chip-sized microelectromechanical system (MEMS)-based FTIR spectrometer. The core optical engine of the solution is built using a passive-alignment integration technique for a selfaligned MEMS chip; self-aligned microoptics and a single detector in a tiny package sized about 1 cm3. The MEMS chip is a monolithic, high-throughput scanning Michelson interferometer fabricated using deep reactive ion etching technology of silicon-on-insulator substrate. The micro-optical part is used for conditioning the input/output light to/from the MEMS and for further light direction to the detector. Thanks to the all-reflective design of the conditioning microoptics, the performance is free of chromatic aberration. Complemented by the excellent transmission properties of the silicon in the infrared region, the integrated solution allows very wide spectral range of operation. The reported sensor’s spectral resolution is about 33 cm-1 and working in the range of 1270 nm to 2700 nm; upper limited by the extended InGaAs detector. The presented solution provides a low cost, low power, tiny size, wide wavelength range NIR spectral sensor that can be manufactured with extremely high volumes. All these features promise the compatibility of this technology with the forthcoming demand of smart portable and IoT devices.
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